7MbAbstractThe effect of thermal treatments on the lattice of Zeolite Y and on intracrystalline non lattice material is investigated by solid state magic angle spinning NMR. (^29)Si and (^27)Al NMR show that large amounts of both silicon and aluminium are dislodged from the lattice by calcination and steaming treatments. Non lattice material is readily observed by (^29)Si CP/MAS; the presence of such material may also be deduced from the single pulse spectra by means of spectral deconvolution techniques.
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